Reappraisement and refinement of zircon U-Pb isotope and trace element analyses by LA-ICP-MS | |
Chen HaiHong; Xu Juan; Gao Shan; Gao ChangGui; Zong KeQing; Hu ZhaoChu; Liu YongSheng | |
2010 | |
发表期刊 | CHINESE SCIENCE BULLETIN |
卷号 | 55期号:15页码:1535-1546 |
摘要 | A protocol was established for simultaneous measurements of zircon U-Pb ages and trace elements by LA-ICP-MS at spot sizes of 16-32 mu m. This was accomplished by introducing N(2) into ICP to increase the sensitivity. The obtained U-Pb ages for zircon standards GJ-1, TEMORA and SK10-2 are consistent with the preferred values within about 1% uncertainty (2s) by simple external calibration against zircon standard 91500. Different data reduction softwares could yield different uncertainties for calculation of U-Pb ages. The commercially available program GLITTER4.4 could apply an improper uncertainty calculation strategy, but it may yield artificial high precisions for single analyses. Our trace element analyses indicate that Si is not an ideal internal standard for zircon when calibrated against the NIST glasses. Calibration against the NIST glasses using Si as an internal standard, a systematic deviation of 10%-30% was found for most trace elements including Zr. However, the trace element compositions of zircon can be accurately measured by calibration against multiple reference materials with natural compositions ( e. g., BCR-2G, BHVO-2G and BIR-1G), or calibration against NIST SRM 610 and using Zr as an internal standard. Analyses of two pieces of GJ-1 demonstrate that it is relatively homogenous for most trace elements (except for Ti). |
关键词 | Zircon U-Pb age trace element uncertainty LA-ICP-MS |
DOI | 10.1007/s11434-010-3052-4 |
语种 | 英语 |
ISSN | 1001-6538 |
收录类别 | SCI ; ESI高被引论文 |
WOS记录号 | WOS:000278704100011 |
WOS类目 | Multidisciplinary Sciences |
出版者 | SCIENCE PRESS |
出版地 | 16 DONGHUANGCHENGGEN NORTH ST, BEIJING 100717, PEOPLES R CHINA |
引用统计 | |
文献类型 | 期刊论文 |
条目标识符 | http://ir.cug.edu.cn/handle/2XU834YA/279143 |
专题 | 教学院系_环境学院 |
通讯作者 | Liu YongSheng |
作者单位 | 1.China Univ Geosci, Fac Earth Sci, State Key Lab Geol Proc & Mineral Resources, Wuhan 430074, Peoples R China. 2.NW Univ Xian, Dept Geol, State Key Lab Continental Dynam, Xian 710069, Peoples R China. |
推荐引用方式 GB/T 7714 | Chen HaiHong,Xu Juan,Gao Shan,et al. Reappraisement and refinement of zircon U-Pb isotope and trace element analyses by LA-ICP-MS[J]. CHINESE SCIENCE BULLETIN,2010,55(15):1535-1546. |
APA | Chen HaiHong.,Xu Juan.,Gao Shan.,Gao ChangGui.,Zong KeQing.,...&Liu YongSheng.(2010).Reappraisement and refinement of zircon U-Pb isotope and trace element analyses by LA-ICP-MS.CHINESE SCIENCE BULLETIN,55(15),1535-1546. |
MLA | Chen HaiHong,et al."Reappraisement and refinement of zircon U-Pb isotope and trace element analyses by LA-ICP-MS".CHINESE SCIENCE BULLETIN 55.15(2010):1535-1546. |
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